An <i>in situ</i> liquid environment for synchrotron hard X-ray nanoprobe microscopy

Studying chemical reactions in an environment that closely mimics the system’s natural operating conditions can offer crucial insights into dynamic oxidation processes. Transmission Electron Microscopes (TEMs) and X-ray Nanoprobes allow use of imaging spectroscopy to access nanoscale structural information about these However, controlled constraints make design implementation situ sample environments challenging. Here, we outline setup liquid for Hard Nanoprobe beamline (I14) at Diamond Light Source. The allows spectroscopic analysis samples exposed flow, with heating up 80℃. capability is demonstrated example experiment studying iron corrosion. cell offers prospect combining electron microscopy multi-length scale liquid.